research proposal
TRANSCRIPT
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Rasulullah s.a.w. bersabda: “Sesungguhnya telah diturunkan kepadaku pada waktu malam sebuah Surah yang aku cintai lebih dari dunia ini dan isinya.” Pada
riwayat yang lain, “yang lebih aku cintai daripada apa yang disinari oleh cahaya matahari.” Dan kemudian baginda membaca: “Innaa fatahnaa laka fatham
mubiinaa (ayat pertama Surah al-Fath).” (Riwayat Bukhari)
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REDUCTION REACTION OF PLATINUM NANOPARTICLE
WITH PALM LEAVES EXTRACT
PRESENTED BY:NOR AIN BINTI RAMLI
2012770949
SUPERVISOR:MDM.NOORSUHANA MOHD YUSOF
CO-SUPERVISOR:DR. JUNAIDAH JAI
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Introduction
Why we do this research?
Despite for green production of nanoparticles
Issues on worldwide problems associcted with environmental
contamination
Despite for green chemistry
&nanotechnology
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Advantages of Greener Technology
Environmental
friendly
Non-Toxic
Low cost based on technology , application &
sources
Simple yet fast
processing technique
Clean
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Platinum (Pt)
Nanoparticles
Applications
Catalyst TechnologyDevelopment
Medical Therapy Application
Nanotechnology
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Catalyst Technology
Start with problem Fuel sell powered vehicles that run from hydrogen
How to produce the hydrogen cheaper & how to store it safely
Problem solver (Researchers)Form of new catalyst: Platinum nanoparticles
Problems:-Expensive -can be easily deactivated in the presence off low levels of carbon monoxide rendering the fuel cell inoperable
Resolution Catalyst using platinum nano particles deposited on a support material of titanium oxide.
Added tungsten to increase the electrical conductivity of the catalyst
Result: Platinum catalyst is 2,000 times more resistant to carbon monoxide
Alternative fossil fuel
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Various devastated sources for the preparation of nanoparticles
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Previous Research
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Problem Statements 3) Comprehensive study on kinetic and extend of reaction and any others condition that yield to the product Platinum nanoparticles.
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Research Objective
To extract the oil palm leaves at specific condition of temperature and time due to drying process.
To investigate the kinetic, yield as well as extend of reaction of the synthesis Platinum (Pt) nanoparticles.
To comprehend the reaction mechanism involved in synthesis of Platinum aqueous solution to produced Platinum nanoparticles.
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Research Methodology
Extraction of
oil palm
leaves
Characterization of the oil palm
leaves extract
Synthesis of platinu
m nanoparticle
s
Investigation
of kinetic
s, extent
of reaction and yield
of platinu
m nanoparticle
s
Characterization of platinu
m nanoparticle
s
Papers and report writing
Source: (K. Raja, et al., 2012)
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Collecting matured oil palm leaves
Washing the leaves with the running tab water then shred the washed leaves into small pieces
Heat the shredded leaves with distilled water (ratio of leaves to distilled water, temperature and heating time will be investigated)
Filter the solution and collect the oil palm leaves extract for the synthesis (composition of the extract will be evaluated using GC-MS and FTIR)
Synthesis of Pt nanoparticles (reduction temperature and time will be investigated)
FTIR & XRD (identify the purity of the Pt
nanoparticles)
UV-vis (identify the extant of reaction, kinetic and yield)
SEM and TEM (identify the shape and the size of the
nanoparticles)
Flow Chart of Research Activities
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Expected Results
Able to develop the knowledge on the
kinetic and extend of reaction of yield platinum (Pt)
synthesis using palm leaves extract
Able to comprehend
the mechanism of reduction and capping agent in synthesis of platinum (Pt)
nanoparticles using palm
leaves extarct
Able to understand the application of palm leaves extract in the synthesis of
platinum nanoparticles
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Gantt Chart of Research Activities
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Milestone &Dates of Research Activities
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Thank You Seek for advice