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8/10/2019 LAPORAN CUSO4.5H2O.doc

1/16

LAPORAN PRAKTIKUM SATUAN PROSES

PEMBUATAN CuSO4.5H2O

Oleh

DILA ADILA NIM 131411059

RIMA AGUSTIN M NIM 131411061

ULFA NURUL A NIM 131411063

Dosen Pembimbin !

I"# $mm%n&el% M%"i% 'i()%n*i+ MT

PROGRAM STUDI DIII TEKNIK KIMIA

JURUSAN TEKNIK KIMIA

POLITEKNIK NEGERI BANDUNG

2014


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A. LANDASAN TEORI

Temb%% %(%l%h lo%m me"%h , m&(% )%n l&n%-+ (%.%* (i*em.% (%n (ili%*# Temb%%

meleb&" .%(% 103/0# %"en% .o*ensi%l ele-*"o(% s*%n(%" .osi*i2+ 0+34 ol* &n*&- .%s%n%n

& &78+ i% *i(%- l%"&* (%l%m %s%m -lo"i(% (%n %s%m s&l2%* ene" mes-i.&n (en%n %(%n)%

o-sien i% l%"&* se(i-i*# N%m&n+ %s%m ni*"%* (en%n m&(%h mel%"&*-%n *emb%% -%"en% %s%m

ni*"%* me"&.%-%n .el%"&* sem&% lo%m -e&%li em%s (%n .l%*in%# :e"i-&* "e%-si )%n *e";%(i !

3& /% ,

sen)%>% ini *i(%- be">%"n%+ -eb%n)%-%n %"%m *emb%% I8 *%- l%"&* (%l%m %i"+ m&(%h

(io-si(%si men;%(i sen)%>% *emb%% II8+ )%n (%.%* (i*&"&n-%n (%"i *emb%% II8 o-si(%+

&O+ hi*%m# G%"%m ,%"%m *emb%% II8 &m&mn)% be">%"n% bi"&+ b%i- (%l%m ben*&- hi("%*+

.%(%*+ m%&.&n (%l%m l%"&*%n %i"+ >%"n% ini ben%" ,ben%" -h%s h%n)% &n*&- ion -om.le-s

*e*"%-&o-&."%* II8+ )%i*& >%"n% ion *emb%% II8 (%l%m l%"&*%n %i"# G%"%m , %"%m *emb%%II8 %nhi("%*+ se.e"*i *emb%% II8 s&l2%* %nhi("%* &SO4+ be">%"n% .&*ih %*%& se(i-i* -&nin#

D%l%m l%"&*%n %i" sel%l& *e"(%.%* ion -om.le-s *e*"%%-&o (%l%m ."%-*e- h%n)% ion *emb%%

II8 )%n .en*in#

D%l%m s&%*& Sis*em Pe"io(i- Uns&" SPU8+ *emb%% &8 *e"m%s&- -e (%l%m

olon%n 11# Temb%%+ .e"%- (%n em%s (iseb&* lo%m -oin -%"en% (i.%-%i se;%- l%m%

seb%%i &%n (%l%m ben*&- lem.en%n -oin8# %-*& )%n l%m%# Temb%% %(%l%h lo%m be"(%)%

h%n*%" lis*"i- *ini+ m%-% (i.%-%i seb%%i -%bel lis*"i-# Temb%% *i(%- l%"&* (%l%m %s%m )%n

b&-%n .eno-si(%si *e*%.i *emb%% *e"o-si(%si oleh


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.%(% 110 @ (%n -elim%=lim% mole-&l %i" .%(% 150 @# P%(% 650 @+ *emb%% II8 s&l2%*

men&"%i men;%(i *emb%% II8 o-si(%&O8+s&l2&" (io-si(%SO78 (%no-sienO78 #

Temb%% &8 me"&.%-%n s%l%h s%*& lo%m )%n .%lin "in%n (%n .%lin %-*i2# &

men%l%mi (is."o.o"sion%si se%"% s.on*%n .%(% -e%(%%n s*%n(%" b%-&8# % *emb%% l%inn)%#

Sen)%>% ini ;&% (i&n%-%n (%l%m .en)e.&h%n (%n .e>%"n%%n *e-s*il se"*% seb%%i b%h%n

.en%>e* -%) :en*&- %nhi("%*n)% (i&n%-%n &n*&- men(e*e-si %i" (%l%m ;&ml%h -el&mi*#

Temb%% s&l2%* ;&% (i-en%l seb%%i Bi*"iol bi"

Temb%% II8 s&l2%* me"&.%-%n .%(%*%n -"is*%l bi"&+ &SO4#5


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B. TUJUAN PERCOBAAN

Se*el%h mem.el%;%"i (%n mel%-&-%n .e"ob%%n ini m%h%sis>% (ih%"%.-%n m%m.& !

%# Memb&%* -"is*%l *emb%% II8 s&l2%* .en*%hi("%* (%"i limb%h *emb%%

b# Menen%l si2%*=si2%* -"is*%l *emb%% II8 s&l2%* .en*%hi("%*# Men%n%lisis ."o(&- (en%n menhi*&n "en(em%n (%n ;&ml%h %i" -"is*%l hi("%*8 se%"%

s*oi-hiome*"i

C. ALAT DAN BAHAN

ALAT SPESIFIKASI JUMLAH BAHAN SPESIFIKASI JUMLAH

Hot p!t" 1 L%"&*%n


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D. SKEMA KERJA

E. DATA PENGAMATAN

%>%n .o"selen -oson E 51+4 "%m

%% %"lo;i -oson E 43+00 "%m

%% %"lo;i -"is*%l &SO4#5%n .o"selen s%m.el &SO4#5


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F. PENGOLAHAN DATA

Di-e*%h&i ! M%ss% & E 5 "%m

M%ss% "is*%l E 14+7/ "%m

:M &SO4#5


7/16

Mol &SO4#5


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M"&'o)$%(!$% Cu *"&''u&!)!& HNO p")!t

3&s8 /%"n% o-l%*# U%. ini *e"ben*&- seb%%i %-ib%*

*emb%% )%n (i"e%-si-%n (en%n %s%m ni*"%* .e-%*# %"en% .%(% .e"ob%%n ini

(i.e"l&-%n >%-*& )%n *i(%- se(i-i* (%"i "e%-si %n*%"% *emb%% (%n %s%m ni*"%* .e-%*+

m%-% (%l%m ."oses ini (i.e"l&-%n .en%(&-%n s%m.%i sel&"&h *emb%% l%"&*# Pe"s%m%%n

"e%-sin)% %(%l%h seb%%i be"i-&* !

3& /%"n% bi"& -e"&h se"*% *e"(%.%* &%.

be">%"n% o-l%* *&%# U%. ini *e"ben*&- seb%%i %-ib%* (%"i *emb%% )%n (i"e%-si-%n

(en%n %s%m ni*"%* .e-%* (%n %s%. ini me"&.%-%n %s NO# D%l%m ."oses ini -i*% l%-&-%n

.en%(&-%n se(i-i* lebih l%m%+ -%"en% -i*% l%-&-%n .en%(&-%n s%m.%i *emb%% bene"=


10/16

ben%" l%"&*# Sehin%n)% .%(% .e"ob%%n ini+ -e.in%n *emb%% )%n -i*% .%-%i h%"&s

(i.o*on se-eil m&n-in#

P"ose(&" sel%n;&*n)% se*el%h .en%mb%h%n bebe"%.% sen)%>% (i%*%s+ %m.&"%n

(i.%n%s-%n (en%n *&;&%n &n*&- mem.e"e.%* ."oses "e%-si# Sel%in i*&+ *&;&%n (%"i

.em%n%s%n ini %(%l%h &n*&- mem.e"bes%" h%sil -%li (%"i ion=ionn)% (%n mem.e"-eil

h%"% h%sil -%li -el%"&*%nn)% s.8+ sehin% h%l ini (%.%* memben*&- en(%.%n -"is*%l#

"is*%l )%n *e"ben*&- inil%h )%n (in%m%-%n *emb%% II8 s&l2%*# P"oses .em%n%s%n ini

sen(i"i -i*% hen*i-%n -e*i-% %s s&(%h be">%"n% o-l%* m&(%#

Pe"s%m%%n "e%-si )%n se%"% len-%.n)% %(%l%h seb%%i be"i-&*!

& 3%"n% bi"& *&% (en%n

en(%.%n )%n men%n(&n ?%* .eno*o"8 be">%"n% bi"& m&(%# Se*el%h i*&+ 2il*"%* )%n

*el%h (is%"in (i(inin-%n (i(%l%m e-si-%*o" &n*&- men(%.%*-%n -"is*%l (%"i *emb%%

II8 s&l2%*#

Pe"s%m%%n "e%-si )%n be"l%ns&n %(%l%h seb%%i be"i-&*!

&NO387


11/16

Pe"s%m%%n "e%-si )%n *e";%(i %(%l%h seb%%i be"i-&*!

&73


12/16

(en%n en(%.%n )%n men%n(&n ?%* .eno*o"8 be">%"n% hi;% Sel%n;&*n)%+ 2il*"%*

)%n *el%h (is%"in (i(i%m-%n sel%m% s%*& h%"i &n*&- men(%.%*-%n -"is*%l (%"i *emb%%

II8 s&l2%*# Pe"s%m%%n "e%-sin)% %(%l%h seb%%i be"i-&*!

&NO387 %"n% bi"& -e"&h se"*% *e"(%.%* &%. be">%"n% o-l%*#U%. ini *e"ben*&- seb%%i %-ib%*

(%"i *emb%% )%n (i*%mb%h-%n %*%& (i"e%-si-%n (en%n %s%m ni*"%* .e-%* memben*&-

%s ni*"%*# %"en% (i.e"l&-%n >%-*& )%n *i(%- se(i-i* (%"i "e%-si %n*%"% *emb%% (%n


13/16

%s%m ni*"%* .e-%*+ m%-% (%l%m ."oses ini (i.e"l&-%n .en%(&-%n s%m.%i sel&"&h

*emb%% l%"&*# Pe"s%m%%n "e%-sin)% %(%l%h seb%%i be"i-&* !

& 4 %"n% bi"& *&% (en%n en(%.%n )%n

men%n(&n ?%* .eno*o"8 be">%"n% %%- -ehi;%&%n# Sel%n;&*n)%+ 2il*"%* )%n *el%h

(is%"in (i(i%m-%n sel%m% s%*& h%"i &n*&- men(%.%*-%n -"is*%l (%"i *emb%% II8 s&l2%*#

Pe"s%m%%n "e%-sin)% %(%l%h seb%%i be"i-&* !

&NO387 %-*& )%n (i.e"l&-%n &n*&- .emben*&-%n s%n%* se(i-i* sehin% &-&"%n

.%"*i-el lebih -eil# Un*&- men(%.%*-%n -"is*%l )%n m&"ni+ m%-% (il%-&-%n ."oses

.ene"in%n# D%"i ."oses ini (i.e"oleh ?%* )%n (iinin-%n )%n beb%s (%"i ?%* .eno*o"#

P"oses )%n *e";%(i %(%l%h seb%%i be"i-&* !

&73


14/16

.en%mb%h%n %s%m ni*"%* -e(%l%m l%"&*%n )%n lebih se(i-i* (%"i.%(% seh%"&sn)% ;&%

mem.en%"&hi be"%* (%"i -"is*%l *e"seb&*#

I. MATERIAL SAFET9 DATA SHEET

T"*8!'!:II; $u

N!*! IUPAC

Temb%%II8 s&l2%*

N%m% l%in

&."i s&l2%*

i*"iol bi"& .en*%hi("%*8

:%*& bi"& .en*%hi("%*8

:on%*i* mine"%l *"ihi("%*8

:o*i* mine"%l he.*%hi("%*8

%l-%n*i*mine"%l .en*%hi("%*8

%l-osi%ni* mine"%l8

I("&t%

Pen%m.il%nbi"& .en*%hi("%*8

%b&=%b& .&*ih %nhi("%*8

Densi*%s3#603 m3%nhi("%*8

7#7/4 m3.en*%hi("%*8

Ti*i- leb&" 110 @ 4


15/16

650 @ decomp.

el%"&*%n(%l%m %i"

pentahydrate

316 L 0 @8

7033 L 100 @8

form unspecified

370 L 70 @861/ L 60 @8

1140 L 100 @8

el%"&*%n

anhidrat

*i(%- be"%m.&" .%(% e*%nol

pentahidrat

be"%m.&" (i me*%nol

10#4 L 1/ @8

*i(%- be"%m.&" (ie*%nol

In(e-s bi%snD8 1#514 .en*%hi("%*8

St#u)tu#

S*"&-*&" -"is*%l

O"*ho"hombih%lo)%ni*e8+s.%e "o&.Pnm%+ oP74+% E 0#/39

nm+ b E 0#669 nm+ E 0#4/3 nmK1

T"ilini.en*%h)("%*e8+s.%e

"o&.P1+ %P77+ % E 0#59/6 nm+ b

E 0#6141 nm+ E 1#036 nm+ E

#333@+ Q E /7#76@+ E 7#56@K7

T"#*o)%*%!

$n*"o.i mol%"

s*%n(%"So79/109#05 1 mol1

B!-!6!

MSDS %nh)("o&s.en*%h)("%*e

l%si2i-%si $U

:e"%&n =&8

I"i*%si =%8

:e"b%h%)% b%i lin-&n%n N8

In(e-s $U 079=004=00=0

NFPA 04 0

71

F"%s%=R R77+ R363/+ R5053

F"%s%=S S7+ S77+ S60+ S61

LD50 300 m- o"%l+ "%*8

/ m- o"%l+ mo&se8
http://id.wikipedia.org/wiki/Kelarutanhttp://id.wikipedia.org/wiki/Airhttp://id.wikipedia.org/wiki/Kelarutanhttp://id.wikipedia.org/wiki/Etanolhttp://id.wikipedia.org/wiki/Metanolhttp://id.wikipedia.org/wiki/Etanolhttp://id.wikipedia.org/wiki/Etanolhttp://id.wikipedia.org/wiki/Indeks_biashttp://id.wikipedia.org/wiki/Struktur_kristalhttp://id.wikipedia.org/w/index.php?title=Orthorhombic&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Pearson_symbol&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Pearson_symbol&action=edit&redlink=1http://id.wikipedia.org/wiki/Tembaga(II)_sulfat#cite_note-1http://id.wikipedia.org/w/index.php?title=Triclinic&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Triclinic&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Pearson_symbol&action=edit&redlink=1http://id.wikipedia.org/wiki/Tembaga(II)_sulfat#cite_note-2http://id.wikipedia.org/w/index.php?title=Entropi_molar_standar&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Entropi_molar_standar&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=MSDS&action=edit&redlink=1http://hazard.com/msds/mf/baker/baker/files/c5920.htmhttp://hazard.com/msds/mf/baker/baker/files/c5918.htmhttp://id.wikipedia.org/w/index.php?title=Directive_67/548/EEC&action=edit&redlink=1http://id.wikipedia.org/wiki/NFPA_704http://id.wikipedia.org/wiki/Daftar_frasa_Rhttp://id.wikipedia.org/wiki/Daftar_frasa_Shttp://id.wikipedia.org/w/index.php?title=Dosis_letal_median&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Dosis_letal_median&action=edit&redlink=1http://id.wikipedia.org/wiki/Berkas:NFPA_704.svghttp://id.wikipedia.org/wiki/Kelarutanhttp://id.wikipedia.org/wiki/Airhttp://id.wikipedia.org/wiki/Kelarutanhttp://id.wikipedia.org/wiki/Etanolhttp://id.wikipedia.org/wiki/Metanolhttp://id.wikipedia.org/wiki/Etanolhttp://id.wikipedia.org/wiki/Indeks_biashttp://id.wikipedia.org/wiki/Struktur_kristalhttp://id.wikipedia.org/w/index.php?title=Orthorhombic&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Pearson_symbol&action=edit&redlink=1http://id.wikipedia.org/wiki/Tembaga(II)_sulfat#cite_note-1http://id.wikipedia.org/w/index.php?title=Triclinic&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Space_group&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Pearson_symbol&action=edit&redlink=1http://id.wikipedia.org/wiki/Tembaga(II)_sulfat#cite_note-2http://id.wikipedia.org/w/index.php?title=Entropi_molar_standar&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Entropi_molar_standar&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=MSDS&action=edit&redlink=1http://hazard.com/msds/mf/baker/baker/files/c5920.htmhttp://hazard.com/msds/mf/baker/baker/files/c5918.htmhttp://id.wikipedia.org/w/index.php?title=Directive_67/548/EEC&action=edit&redlink=1http://id.wikipedia.org/wiki/NFPA_704http://id.wikipedia.org/wiki/Daftar_frasa_Rhttp://id.wikipedia.org/wiki/Daftar_frasa_Shttp://id.wikipedia.org/w/index.php?title=Dosis_letal_median&action=edit&redlink=1


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40 m- o"%l+ m%mm%l8

S"&6!>! t"#)!%t

%*ionl%inn)%Ni-elII8 s&l2%*

Sen s&l2%*
http://id.wikipedia.org/wiki/Ionhttp://id.wikipedia.org/w/index.php?title=Nikel(II)_sulfat&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Seng_sulfat&action=edit&redlink=1http://id.wikipedia.org/wiki/Ionhttp://id.wikipedia.org/w/index.php?title=Nikel(II)_sulfat&action=edit&redlink=1http://id.wikipedia.org/w/index.php?title=Seng_sulfat&action=edit&redlink=1

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