june 2003 detergent testing services 211palmoilis.mpob.gov.my/publications/tot/tt197.pdfformulation...

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D D MPOB INFORMATION SERIES ISSN 1511-7871 JUNE 2003 by: MOHTAR YUSOF; ZAHARIAH ISMAIL and SALMIAH AHMAD MPOB TT No. 197 DETERGENT TESTING SERVICES 211 211 211 211 211 Malaysian Palm Oil Board, Ministry of Primary Industries, Malaysia P. O. Box 10620, 50720 Kuala Lumpur, Malaysia. Tel: 03-89259155, 89259775, Website: http: //mpob. gov. my Telefax: 03-89259446 (AC Nielsen, 2003). To maintain the interest and loyalty of consumers who have many choices in the market, detergent companies are introducing more varieties of surfactants and ingredients in their products. Cleaning performance remains an important basic requirement, but subtle quality such as appearances and foaming property are also critical for a successful product. To keep up with the changing market trend, detergent producers are constantly updating their product lines to cater for the needs of consumers of diversed cultural and religious backgrounds. THE IMPORTANCE OF DETERGENT TESTING SERVICES The fundamental questions on detergents are (i) will the product perform and function as claimed by the manufacturer and as expected by the consumer, and (ii) is the buyer getting value for money. Most of the manufacturers continue to sell sub-standard products, so this will force consumers to lose confidence etergents are commonly used in our daily life. In Malaysia, the detergent market value in 2002 was RM 486.5 million with powder formulation constituting 72.5%, liquid 11.6% and bar 15.6%, corresponding to 78 700 t, 11 952 t and 19 600 t respectively in their products and switch to a competitors product. It is important for manufacturers to ensure that product performs as claimed. The detergent testing services are therefore offered to the industry, especially cleaning products manufacturers for an independent body to evaluate the performance of their products and to substantiate claims. DETERGENT TESTING SERVICES A complete analysis of a detergent is a very specialized area requiring many advanced analytical techniques, a good knowledge of the chemistry and physics of the detection methods (Milwidsky and Gabriel, 1994). Currently, detergent formulations tend to be rather complex and this means that highly sophisticated methods are required to give a complete elucidation of their composition. A laboratory has been set up in AOTC, MPOB to provide the analysis of detergents. The laboratory is well equipped to carry out the important quality parameters of detergents. The test of important quality parameters and the cost for each test are indicated in Table 1. Figure 1. Laboratory for detergent testing services.

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Page 1: JUNE 2003 DETERGENT TESTING SERVICES 211palmoilis.mpob.gov.my/publications/TOT/tt197.pdfformulation constituting 72.5%, liquid ... Laundry Detergent 2001 and ... Petaling Jaya. ASTM

DDMPOB INFORMATION SERIES ISSN 1511-7871

JUNE 2003

by: MOHTAR YUSOF; ZAHARIAH ISMAIL and SALMIAH AHMAD

MPOB TT No. 197

DETERGENT TESTINGSERVICES 211 211 211 211 211

Malaysian Palm Oil Board, Ministry of Primary Industries, MalaysiaP. O. Box 10620, 50720 Kuala Lumpur, Malaysia. Tel: 03-89259155, 89259775, Website: http: //mpob. gov. my Telefax: 03-89259446

(AC Nielsen, 2003). To maintain the interest and loyaltyof consumers who have many choices in the market,detergent companies are introducing more varieties ofsurfactants and ingredients in their products. Cleaningperformance remains an important basic requirement, butsubtle quality such as appearances and foaming propertyare also critical for a successful product. To keep up withthe changing market trend, detergent producers areconstantly updating their product lines to cater for theneeds of consumers of diversed cultural and religiousbackgrounds.

THE IMPORTANCE OF DETERGENT TESTING SERVICES

The fundamental questions on detergents are (i) will theproduct perform and function as claimed by themanufacturer and as expected by the consumer, and (ii) isthe buyer getting value for money.

Most of the manufacturers continue to sell sub-standardproducts, so this will force consumers to lose confidence

etergents are commonly used in our dailylife. In Malaysia, the detergent market valuein 2002 was RM 486.5 million with powderformulation constituting 72.5%, liquid11.6% and bar 15.6%, corresponding to 78700 t, 11 952 t and 19 600 t respectively

in their products and switch to a competitor�s product.It is important for manufacturers to ensure that productperforms as claimed.

The detergent testing services are therefore offered to theindustry, especially cleaning products manufacturers foran independent body to evaluate the performance of theirproducts and to substantiate claims.

DETERGENT TESTING SERVICES

A complete analysis of a detergent is a very specializedarea requiring many advanced analytical techniques, agood knowledge of the chemistry and physics of thedetection methods (Milwidsky and Gabriel, 1994).Currently, detergent formulations tend to be rathercomplex and this means that highly sophisticated methodsare required to give a complete elucidation of theircomposition.

A laboratory has been set up in AOTC, MPOB to providethe analysis of detergents. The laboratory is well equippedto carry out the important quality parameters ofdetergents.

The test of important quality parameters and the cost foreach test are indicated in Table 1.

Figure 1. Laboratory for detergent testing services.

Page 2: JUNE 2003 DETERGENT TESTING SERVICES 211palmoilis.mpob.gov.my/publications/TOT/tt197.pdfformulation constituting 72.5%, liquid ... Laundry Detergent 2001 and ... Petaling Jaya. ASTM

Companies needing this service are requested to delivertheir samples with a written instruction stating the test(s)required. All samples received will be checked to ensurethat they are in good condition for the analysis. The resultsof analysis in the form of certificate of analysis will beready in two days to three weeks depending on the typeof analysis.

The invoice will be sent together with the certificate ofanalysis. The company can use the results of analysis toevaluate the performance of his product, whether it issatisfactory or its quality needs to be further improved.

For more information, kindly contact Dr. Mohtar Yusof [email protected] or Dr. Salmiah Ahmad at

TABLE 1. DETERGENT TESTING SERVICES AVAILABLE IN MPOB

Parameter Method of Analysis Cost/test (RM)Washing performance ASTM D 3050-92(1997) 70Foaming property Based on ASTM 30Anti-rust property Based on ASTM 170Type of surfactants Milwidsky and Gabriel (1994)- Anionic, cationic ASTM D 3049-89 (1997) 1 400- Nonionic ASTM D 2959-95 (1997)pH pH meter 20Sodium carbonate Milwidsky and Gabriel (1994) 30Oxidizing agent Milwidsky and Gabriel (1994) 30Chelating agent Milwidsky and Gabriel (1994) 40Carboxymethyl cellulose BS 3762:Section 3.15 30Complex phosphate Milwidsky and Gabriel (1994) 40Chlorine releasing agent Milwidsky and Gabriel (1994) 20Sulphate Milwidsky and Gabriel (1994) 30

[email protected], or at AOTC, MPOB, Lot 9 & 11,Jalan P/14, Seksyen 10, 43650 Bandar Baru Bangi, Selangor.Tel. No. 03-89255708 and Fax No. 03-89256197.

REFERENCES

AC NIELSEN (2003). Historical Annual Data, LaundryDetergent 2001 and 2002. Petaling Jaya.

ASTM (1997). Annual Book of ASTM Standards, Volume15.04, Soap, Polishes, Leather, Resilient Floor Coverings.Danvers.

MILWIDSKY, B M and GABRIEL, D M (1994). DetergentAnalysis. George Godwin, Essex, U.K.

For more information kindly contact:

Director-GeneralMPOB

P. O. Box 1062050720 Kuala Lumpur, Malaysia.

Tel: 03-89259155, 89259775,Website: http: //mpob. gov. my

Telefax: 03-89259446