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46
PANDUAN PERKHIDMATAN MAKMAL MAKANAN KEMENTERIAN KESIHATAN MALAYSIA Oleh KEMENTERIAN KESIHATAN MALAYSIA

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Page 1: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

PANDUAN PERKHIDMATAN MAKMAL MAKANAN

KEMENTERIAN KESIHATAN MALAYSIA

Oleh

KEMENTERIAN KESIHATAN MALAYSIA

Page 2: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

Keupayaan makmal memberikan perkhidmatan analisis adalah

parameter analisis yang diberikan agar keputusan yang

dikeluarkan adalah diterima sepenuhnya.

memerlukan pematuhan sepenuhnya bagi syarat-syarat yang ditetapkan oleh negara

pengimport. Ianya termasuk syarat akreditasi makmal yang menyediakan perkhidmatan

masa hadapan kemaskini keupayaan analisis dan status akreditasi yang terkandung di

dalam buku ini akan dimuatkan di laman web

Maklumat yang terkandung dalam buku ini adalah diharapkan dapat membantu program

negara ini adalah selamat untuk orang ramai.

NORAINI BT. DATO’ MOHD OTHMAN

Kementerian Kesihatan Malaysia

Perutusan Pengarah Kanan

ii

Page 3: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

Perkhidmatan analisis yang ditawarkan

Makmal telah memperolehi akreditasi

KANDUNGAN

i

ii

Muka

surat

F

*

Sidang Pengarang

Perutusan Pengarah Kanan

1.0 Perkhidmatan Analisis dan Akreditasi

Petunjuk :

Page 4: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

2

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Page 5: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

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Page 6: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

4

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Page 7: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

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aly

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urn

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f

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term

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f

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le R

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term

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ino

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nd

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6

Ch

lora

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nic

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term

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f

Ph

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Me

at

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by L

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ph

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ss

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Me

at

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d F

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0g

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ible

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rtio

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Pla

stic

Fro

ze

n

Jo

urn

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f

Ch

rom

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,

87

5 (

20

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Re

fer

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7

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od

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ric

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le /

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h b

all

/

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h c

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/kg

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stic

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orig

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cka

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t p

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tern

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5)

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rbic

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15

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stic /

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ss /

bo

ttle

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rig

ina

l

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cka

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Re

fer

to

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ble

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Re

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ra R

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oo

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AA

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f C

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0 g

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th e

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cka

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e D

ete

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n o

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Page 10: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

8

Bu

tyla

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tyla

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ne

(BH

T)

Oil

Sol

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our

(Prohi

bite

d

Co

lour

)

Pa

ra R

ed

3

mg

/kg

Dim

eth

yl Y

ello

w6

mg

/kg

Su

da

n 1

3

mg

/kg

Su

da

n 2

3 m

g/k

g

Su

da

n 3

6 m

g/k

g

Su

da

n 4

15

mg

/kg

Perm

itted C

olo

ur

Allu

ra R

ed A

C

Am

ara

nth

Brilli

an

t B

lack P

N

Brilli

an

t B

lue

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Ch

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wn

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rmo

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Ery

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sin

e B

S

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en

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F

Gre

en

S

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igo

tin

e

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nce

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nse

t Y

ello

w F

CF

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rtra

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e

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ino

line

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llow

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t A

va

ilab

le

A

(a)

AO

AC

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icia

l M

eth

od

98

3.1

5,

Ch

.47

(b)

AO

AC

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tern

atio

na

l,

16

th E

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lum

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96

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e D

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Syn

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tic A

ntio

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ts

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A &

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in F

ats

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d B

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by H

igh

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rfo

rma

nce

Liq

uid

Ch

rom

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ph

y

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4-0

06

25

0g

10

mg

/kg

10

mg

/kg

Pla

stic /

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gin

al

Pa

cka

gin

g

Re

fer

to

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ble

1 1

0th

Sch

ed

ule

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g.

24

)

(a)

AS

TA

(Am

erica

n S

pic

e

Tra

de

Asso

cia

tio

n)

20

05

(b)

Yo

shio

ka (

2008)

-

Ta

lan

ta.

Vol. 7

4

De

term

ina

tio

n o

f S

yn

the

tic

Co

lou

r in

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od

Usin

g L

iqu

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rom

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gra

ph

y

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Fa

t a

nd

Ed

ible

Oil

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typ

es o

ffo

od

50

0g

As P

urc

ha

se

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C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

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MKA KK

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jad

ua

l 1

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if m

ak

an

an

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9

E0

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Sa

lte

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y U

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Me

tho

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De

term

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tio

n o

f S

ma

ll

Am

ou

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by

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lha

rd T

itra

tio

n,

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lt C

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sa

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fer

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oo

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gu

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85

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f

Fo

rma

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h M

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an

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sh

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Ch

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du

cts

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1 m

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gF

roze

n

Ad

min

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leve

l: 5

mg

/kg

for

pa

sta

an

d

20

mg

/kg

fo

r

fish

Pla

stic /

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gin

al

Pa

cka

gin

g

Sa

cch

arin

Pe

rmitte

d

on

ly in

dri

ed

fru

it,

dri

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pre

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red

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h

& d

rie

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ma

teN

ot

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rmitte

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cch

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-80

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rmitte

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dri

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& d

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itte

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lfu

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ioxid

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( q

ua

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lfu

r D

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( q

ua

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99

0)

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1

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AA

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AA

AA

AA

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cka

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fer

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od

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e D

ete

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atio

n o

f

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ur

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88

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17

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l.II.

Ch

ap

ter

47

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e D

ete

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atio

n o

f

Sa

cch

arin

an

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ma

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hin

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Ch

rom

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25

-10

0

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A

Th

e D

ete

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Sa

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oo

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ph

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NO

TE

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ME

TH

OD

RE

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NC

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E

MA

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MKA KK

KUCHING

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PULAU PINANG

SELANGOR

PAHANG

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ua

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ak

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10

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Th

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lou

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ma

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Wh

ite

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at

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Me

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56

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AO

AC

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ffic

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tassiu

m b

rom

ate

E0

4-0

14

Th

e D

ete

rmin

atio

n o

f O

il

So

lub

le S

yn

the

tic F

oo

d

Co

lou

rs (

Su

da

n I &

IV

) in

foo

d b

y P

ap

er

Ch

rom

ato

gra

ph

y a

nd

UV

/VIS

Sp

ectr

op

ho

tom

ete

r

AO

AC

(1

99

1)

Off

icia

l

Me

tho

ds o

f A

na

lysis

of

AO

AC

In

tern

atio

na

l

Su

da

n I &

IV

)A

E0

4-0

16

Ra

pid

Me

tho

d f

or

Diffe

ren

tia

tio

n o

f G

en

uin

e

an

d Im

ita

tio

n S

ha

rks F

in

Ch

ew

, S

.T.

et

al (1

99

2);

Sin

ga

po

re J

ou

rna

l o

f

Pro

ma

ryIn

du

str

y 2

0 (

2)

Sh

ark

s F

inF

ish

10 m

g/k

g

E0

4-0

17

Th

e D

ete

rmin

atio

n o

f

Pe

rce

nta

ge

So

lub

le S

olid

in

Fo

od

by R

efr

acto

me

try

Inte

rna

tio

na

l T

em

pe

ratu

re

Co

rre

ctio

n T

ab

le,

19

36

.

Int.

Su

ga

r J.

39

, 2

4s,1

93

7

Pe

rce

nta

ge

So

lub

le S

olid

All

typ

es o

ffo

od

Re

fer

to F

oo

d

Re

gu

latio

ns

19

85

E0

4-0

18

Th

e D

ete

rmin

atio

n o

f N

et

Co

nte

nt

in C

an

ne

d P

rod

uct

by D

rain

ed

We

igh

t M

eth

od

La

wre

nce

, J

.F.,

JA

OA

C,

Vo

l 7

1,

No

5,

19

88

Ne

t C

on

ten

tC

an

ne

d F

ish

2 c

an

sN

ot

less t

ha

n

55

% F

ish

A

E0

4-0

19

Th

e M

ea

su

rem

en

t o

fIo

din

e

Co

nte

nt

in Io

dis

ed

Sa

lt

De

Ma

eye

r E

M,

Lo

we

nste

in

FW

and T

hill

y C

H -

“T

he

Co

ntr

ol o

f

En

de

mic

Go

ite

r"

WH

O,

Ge

ne

va

, 1

97

9

Iod

ine

Co

nte

nt

Sa

lt2

50

g1

5 m

g/k

g2

0 -

30

mg

/kg

AA

A

All

typ

es o

ffo

od

Pla

stic /

Ori

gin

al

Pa

cka

gin

g

As P

urc

ha

se

No

t A

va

ilab

le

No

t

Ava

ilab

le

25

0g

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

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UM

WE

IGH

TL

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NT

AIN

ER

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AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

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PE

RM

ITT

ED

PR

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MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.2: a

dit

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ak

an

an

Page 13: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

11

E0

4-0

20

Th

e D

ete

rmin

atio

n o

fIo

din

e

Co

nte

nt

in Io

dis

ed

Sa

lt

Usin

g Io

do

me

tric

Titra

tio

n

(Pe

ars

on

)

Th

e C

he

mic

al A

na

lysis

of

Fo

od

s,

8th

Ed

itio

n

Iod

ine

Co

nte

nt

Sa

lt2

0 m

g/k

g2

0 -

30

mg

/kg

AA

E0

4-0

22

Th

e D

ete

rmin

atio

n o

f

Pe

roxid

e v

alu

e

MP

OB

Te

st

Me

tho

d

p2

:3 :

20

04

- P

ero

xid

e V

alu

e

Pe

roxid

e V

alu

eE

dib

le O

il &

Fat

/ O

ily F

oo

d

No

t

Ava

ilab

le1

0 m

eq

/kg

E0

4-0

24

Th

e D

ete

rmin

atio

n o

f A

cid

Va

lue

MP

OB

Te

st

Me

tho

d

c2

.7:2

00

4 A

cid

Va

lue

:

Fa

tty A

cid

Acid

Va

lue

Re

fer

to F

oo

d

Re

gu

latio

ns

19

85

E0

4-0

25

Th

e D

ete

rmin

atio

n o

f A

ce

tic

Acid

Ha

rold

Eg

an

et

al.,

Pe

ars

on

's

Ch

em

ica

l

An

aly

sis

of

Fo

od

s.1

981

8th

Ed

itio

n

Ace

tic A

cid

Asp

art

am

e2

50

g/m

l1

00

mg

/kg

Ph

en

yla

lan

ine

25

0g

/ml

10

mg

/kg

(a)

Jo

urn

al o

f F

oo

d

Hyg

ien

e S

ocie

ty o

f Ja

pa

n,

Vo

l. 3

3:

, 1

99

2.

(b)

Ra

pid

An

aly

sis

Me

tho

ds

for

Pe

sticid

e R

esid

ue

s,

Hyg

ien

e a

nd

Ch

em

istr

y,

No

. 4

8,

Ap

ril 8

,19

97

.

As P

urc

ha

se

De

term

ina

tio

n o

f

Asp

art

am

e a

nd

Ph

en

yla

lan

ine

in

So

ft D

rink

by H

igh

Pe

rfo

rma

nce

Liq

uid

Ch

rom

ato

gra

ph

y

E0

4-0

26

Pla

stic /

Ori

gin

al

Pa

cka

gin

g

A

25

0g

So

ft D

rin

k

No

t

Ava

ilab

le2

50

gE

dib

le O

il &

Fat

/ O

ily F

oo

d

No

t A

va

ilab

le

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.2: a

dit

if m

ak

an

an

Page 14: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

12

E0

4-0

31

Th

e D

ete

rmin

atio

n o

f

Synth

etic A

ntioxid

ant

(PG

, T

BH

Q, B

HA

& B

HT

) in

Ed

ible

Oil

by H

igh

Pe

rfo

rma

nce

Liq

uid

Ch

rom

ato

gra

ph

y

Ma

gd

a R

afe

ca

s,

Fra

nce

sc

Gu

ard

iola

, M

iqu

ei Ille

ra,

Ra

fae

l C

od

on

y &

Jo

se

ph

Bo

ate

lla.

(19

98

).

Jo

urn

al o

f

Ch

rom

ato

gra

ph

y A

Syn

the

tic

An

tio

xid

an

tE

dib

le O

il 2

50

gN

ot

Ava

ilab

le

Re

fer

to

Ta

ble

1,

10

th

Sch

ed

ule

(Re

g.

24

)

As P

urc

ha

se

Pla

stic /

Ori

gin

al

Pa

cka

gin

g

Lo

w e

ne

rgy

so

ft d

rin

k -

60

0 m

g/L

,

Oth

er

low

en

erg

y f

oo

d

30

00

mg

/kg

E0

4-0

28

Th

e D

ete

rmin

atio

n o

f

Su

lph

ur

Dio

xid

e in

Fo

od

An

aly

sis

for

To

tal S

ulp

hite

s

in F

oo

ds b

y u

sin

g r

ap

id

Dis

tilla

tio

n f

ollo

we

d b

y

Re

do

x T

itra

tio

n .

De

Vri

es

et

al. J

AO

AC

V

ol 6

9.

No

5,1

98

6

Su

lfu

r D

ioxid

e

A

ll ty

pe

s o

ffo

od

50

0g

AA

E0

4-0

29

Th

e D

ete

rmin

atio

n o

f

Su

lph

ur

Dio

xid

e in

Fo

od

Mo

nie

r W

illia

ms

(a)

Eg

an

,H e

t a

l.(1

98

1)

Pe

ars

on

's C

he

mic

al

An

aly

sis

of

Fo

od

(8

th.E

d)

(b

) A

OA

C 1

6th

Ed

.,

Vo

l .II (1

99

5),

AO

AC

Off

icia

l M

eth

od

93

2.1

6,

Ch

ap

.47

Su

lfu

r D

ioxid

eA

ll ty

pe

s o

ffo

od

50

0g

AF

A

E0

4-0

30

Th

e D

ete

rmin

atio

n o

f

Pro

pio

nic

Acid

In F

lou

r

Co

nfe

ctio

n

AO

AC

Vo

l 6

4,

No

. 2

,

19

81

Pro

pio

nic

Acid

Bre

ad

an

d F

lou

r

Co

nfe

ctio

ne

ry2

50

g4

00

mg

/kg

20

00

mg

/kg

AA

As P

urc

ha

se

Re

fer

to

Ta

ble

1

(Re

g.

20

)

Pla

stic /

Ori

gin

al

Pa

cka

gin

g

25

0g

/ml

No

t

Ava

ilab

le

E0

4-0

27

De

term

ina

tio

n o

f

Ace

su

lfa

me

K u

sin

g

by

Hig

h P

erf

orm

an

ce

Liq

uid

Ch

rom

ato

gra

ph

y

Ace

su

lfa

me

Po

tassiu

mB

eve

rag

es

Eu

rop

ea

n

Sta

nd

ard

EN

12

86

5

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

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CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.2: a

dit

if m

ak

an

an

Page 15: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

13

Nirite

Nitra

te

E0

4-0

33

Th

e D

ete

rmin

atio

n o

f

Me

lam

ine

in

Fo

od

by L

iqu

id

Ch

rom

ato

gra

ph

y T

an

de

m

Ma

ss S

pe

ctr

om

etr

y

(LC

-MS

/MS

)

US

DA

/CF

SA

N.

20

07

.

La

bo

rato

ryIn

form

atio

n

Bu

lletin

No

. 4

39

6,

Vo

lum

e 2

3

Me

lam

ine

All

typ

es o

f fo

od

25

0g

0.0

1

mg

/kg

No

t P

erm

itte

dA

E0

4-0

34

De

term

ina

tio

n o

f

Fo

rma

lde

hyd

e in

Fis

h &

Fis

h P

rod

ucts

an

d P

asta

usin

g N

ash

'sM

eth

od

Be

nja

ku

l e

t.a

l. F

oo

d

Hyd

roco

lloid

s 1

9(2

00

5)

Fo

rma

lde

hyd

eF

ish

an

d F

ish

Pro

du

cts

1 k

g8

.5

mg

/kg

No

t A

va

ilab

le

E0

4-0

36

De

term

ina

tio

n o

f C

itra

te in

Fis

h a

nd

Fis

h P

rod

ucts

usin

g Io

n C

hro

ma

tog

rap

hy

US

En

vir

on

me

nta

l

Pro

tectio

n A

ge

ncy

(EP

A M

eth

od

90

56

A),

Re

v.

, 1

No

v.

20

00

Citra

teF

ish

an

d F

ish

Pro

du

cts

30

0g

25

mg

/kg

No

t A

vaila

ble

AF

Fo

od

Re

gu

latio

ns

19

85

(1

47

) :

EU

reg

ula

tio

ns:

Su

rim

i:

10

00

mg

/kg

,

Oth

er

Fis

h

Pro

du

cts

:

50

00

mg

/kg

As P

urc

ha

se

Pla

stic /

Ori

gin

al

Pa

cka

gin

gF

roze

n

US

En

vir

on

me

nta

l

Pro

tectio

n A

ge

ncy

(EP

A M

eth

od

90

56

A),

Re

v.

1,

No

v.

20

00

E0

4-0

32

De

term

ina

tio

n o

f N

itri

te a

nd

Nitra

te in

Me

at

Pro

du

ct

usin

g Io

n C

hro

ma

tog

rap

hy

Me

at

an

d M

ea

t

Pro

du

cts

30

0g

30

0g

37

5

mg

/kg

Fro

ze

n

50

mg

/kg

20

0 m

g/k

g

To

tal N

itrite

&

Nitra

te

ca

lcu

late

d a

s

Na

triu

m N

itrite

E0

4-0

38

De

term

ina

tio

n o

f

Po

lyp

ho

sp

ha

te in

Fis

h a

nd

Fis

h P

rod

ucts

usin

g Io

n

Ch

rom

ato

gra

ph

y

Po

lyp

ho

sp

ha

teF

ish

an

d F

ish

Pro

du

cts

US

En

vir

on

me

nta

l

Pro

tectio

n A

ge

ncy

(EP

A M

eth

od

90

56

A),

Re

v.

1,

No

v.

20

00

AF

DO

C.

NO

TE

ST

ME

TH

OD

R

EF

ER

EN

CE

PA

RA

ME

TE

RF

OO

D M

AT

RIX

MIN

IMU

M

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.2: a

dit

if m

ak

an

an

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14

jad

ua

l 1

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resid

u r

ac

un

per

osa

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NO

TE

ST

ME

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GROUPR

EF

ER

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RA

ME

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IGH

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(m

g/k

g)

C

ON

TA

INE

RT

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NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

Azin

ph

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thyl

0.0

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fer

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gu

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01

Mu

ltip

le

Sim

ulta

ne

ou

s

Me

tho

d f

or

Pe

sticid

e

Re

sid

ue

s in

Fru

its

an

d V

eg

eta

ble

s

Fre

sh

Fru

its &

Ve

ge

tab

les

1 k

gA

mb

ien

t

Te

mp

era

ture

Bro

wn

pa

pe

r /

pla

stic

Page 17: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

15

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

2,4

-DD

T0

.02

5A

4,4

-DD

D0

.02

5A

4,4

-DD

E0

.02

5A

4,4

-DD

T0

.02

5A

Ald

rin

0.0

25

Ca

pta

fol

0.2

5

Ca

pta

n0

.25

Dic

hlo

ran

0.0

15

A

Die

ldrin

0.0

1A

En

drin

0.0

1A

Gam

ma-H

CH

/

Lin

da

ne

0.0

5A

He

pta

ch

lor

0.0

05

A

Qu

into

ze

ne

0.0

05

A

Tria

de

me

fon

0.0

5

Triflu

mu

ron

0.5

A

Cyflu

thrin

0.2

5A

Cyp

erm

eth

rin

0.0

5A

Fe

nva

lera

te0

.05

A

Pe

rme

thrin

0.0

25

A

Be

nd

ioca

rb0

.02

Ca

rba

ryl

0.2

Ca

rbo

fura

n0

.1

Fe

no

bu

ca

rb0

.12

5

Me

pro

nil

0.5

Pro

po

xu

r0

.25

Th

iob

en

ca

rb0

.01

Jo

urn

al o

f F

oo

d H

yg

ien

e

So

cie

ty o

f Ja

pa

n,

Vo

l.

44

, N

o.

5

Bro

wn

pa

pe

r /

pla

stic

Am

bie

nt

Te

mp

era

ture

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

Organochlorine S.Pyrethroid

Fre

sh

Fru

its &

Ve

ge

tab

les

1 k

g

Carbamate

F0

4-0

01

Mu

ltip

le

Sim

ulta

ne

ou

s

Me

tho

d f

or

Pe

sticid

e

Re

sid

ue

s in

Fru

its

an

d V

eg

eta

ble

s

DO

C.

NO

TE

ST

ME

TH

OD

GROUPR

EF

ER

EN

CE

PA

RA

ME

TE

RF

OO

DM

AT

RIX

MIN

IMU

M

WE

IGH

TL

OQ

(m

g/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

Page 18: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

16

Azin

ph

os e

thyl

0.0

25

Ca

rbo

fen

oth

ion

0.1

Ch

lorp

yri

ph

os

0.0

25

Ch

lorp

yrifo

s m

eth

yl

0.0

25

Cya

no

fen

ph

os

0.0

25

Dia

zin

on

0.0

1

Dic

hlo

rvo

s0

.02

5

Dim

eth

oa

te0

.02

5

Eth

ion

0.0

25

Fe

nitro

thio

n0

.02

5

Fe

nsu

lfo

thio

n0

.01

Fe

nth

ion

0.0

25

Fo

rmo

thio

n0

.02

5

Ma

lath

ion

0.0

2

Me

tha

mid

op

ho

s0

.02

5

Me

thid

ath

ion

0.0

1

Pa

rath

ion

eth

yl

0.0

5

Pa

rath

ion

me

thyl

0.0

5

Ph

osa

lon

e0

.05

Pirim

iph

os m

eth

yl

0.0

1

Pro

fen

op

ho

s0

.02

5

Pro

thio

ph

os

0.0

25

Qu

ina

lph

os

0.0

2

To

lclo

ph

os m

eth

yl

0.0

25

Jo

urn

al o

f F

oo

d H

yg

ien

e

So

cie

ty o

f Ja

pa

n,

Vo

l.3

3,

No

.6

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

Organophosporus

1 k

gO

nio

n,

Ga

rlic

&

Sh

allo

t

Bro

wn

pa

pe

r /

pla

stic

F0

4-0

02

Mu

ltip

le

Sim

ulta

ne

ou

s

Me

tho

d f

or

Pe

sticid

e

Re

sid

ue

s in

Ve

ge

tab

les

(Fro

ze

n M

eth

od

)

Am

bie

nt

Te

mp

era

ture

DO

C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

Page 19: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

17

2,4

-DD

T0

.02

5

4,4

-DD

D0

.02

5

4,4

-DD

E0

.02

5

4,4

-DD

T0

.02

5

Ald

rin

0.0

25

Ca

pta

fol

0.2

5

Ca

pta

n0

.25

Dic

hlo

ran

0.0

15

Die

ldrin

0.0

1

En

drin

0.0

1

γ-H

CH

/Lin

da

ne

0.0

5

He

pta

ch

lor

0.0

05

Qu

into

ze

ne

0.0

05

Tria

de

me

fon

0.0

5

Triflu

mu

ron

0.5

Cyflu

thrin

0.2

5

Cyp

erm

eth

rin

0.0

5

Fe

nva

lera

te0

.05

Pe

rme

thrin

0.0

25

Be

nd

ioca

rb0

.02

Ca

rba

ryl

0.2

Ca

rbo

fura

n0

.1

Fe

no

bu

ca

rb0

.12

5

Me

pro

nil

0.5

Pro

po

xu

r0

.25

Th

iob

en

ca

rb0

.01

Jo

urn

al of

Fo

od

Hyg

ien

e S

ocie

ty o

f

Ja

pa

n,

Vo

l.3

3,

No

.6

Am

bie

nt

Te

mp

era

ture

F0

4-0

02

Mu

ltip

le

Sim

ulta

ne

ou

s

Me

tho

d f

or

Pe

sticid

e

Re

sid

ue

s in

Ve

ge

tab

les

(Fro

ze

n M

eth

od

)

Carbamate

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

1 k

g

Organochlorine S.Pyrethroid

On

ion

, G

arl

ic &

Sh

allo

t

Bro

wn

pa

pe

r /

pla

stic

DO

C.

NO

TE

ST

ME

TH

OD

GROUPR

EF

ER

EN

CE

PA

RA

ME

TE

RF

OO

D M

AT

RIX

MIN

IMU

M

WE

IGH

TL

OQ

(m

g/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

Page 20: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

18

Ch

lorp

yri

ph

os

0.0

05

AA

Ch

lorp

yrifo

s m

eth

yl

0.0

25

A

Cya

no

fen

ph

os

0.0

5A

A

Dia

zin

on

0.0

1A

A

Dic

hlo

rvo

s0

.02

5A

Dim

eth

oa

te0

.02

5

Eth

ion

0.0

25

AA

Fe

nitro

thio

n0

.02

5A

Fe

nsu

lfo

thio

n0

.1

Fe

nth

ion

0.0

25

Fo

rmo

thio

n0

.02

5A

A

Ma

lath

ion

0.0

2A

A

Me

tha

mid

op

ho

s0

.02

5

Me

thid

ath

ion

0.0

25

AA

Pa

rath

ion

eth

yl

0.0

05

Pa

rath

ion

me

thyl

0.0

5A

Ph

en

toa

te0

.02

5

Ph

osa

lon

e0

.05

AA

Pirim

iph

os m

eth

yl

0.0

1A

A

Pro

fen

op

ho

s0

.02

5A

A

Qu

ina

lph

os

0.2

AA

Pro

thio

ph

os

0.0

25

A

To

lclo

ph

os m

eth

yl

0.0

5A

A

Fo

od

Hyg

ien

e S

ocie

ty

of

Ja

pa

n,

Vo

l. 4

4,

No

. 5

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

Am

bie

nt

Te

mp

era

ture

Bro

wn

pa

pe

r /

pla

stic

Mu

ltip

le

Sim

ulta

ne

ou

s

Me

tho

d f

or

Pe

sticid

e

Re

sid

ue

s in

Ce

rea

l,

Be

an

an

d S

ee

ds

F0

4-0

03

Organophosporus

Ce

rea

l, S

ee

ds &

Be

an

s1

kg

DO

C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

Page 21: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

19

DO

C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

Page 22: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

20

F0

4-0

11

De

term

ina

tio

n o

f

Dith

ioca

rba

ma

te in

Ve

ge

tab

le b

y G

as

Ch

rom

ato

gra

ph

y-

Ma

ss S

pe

ctr

om

etr

y

Jo

urn

al o

f A

OA

C

Inte

rna

tio

na

l, 8

3 (

3)

0.0

5

F0

4-0

14

0.0

3A

Azin

ph

os e

thyl

0.0

21

A

Ca

rbo

fen

oth

ion

0.0

35

A

Ch

lorp

yri

ph

os

0.0

11

-0.0

35

AA

Ch

lorp

yrifo

s m

eth

yl

0.0

35

A

Cya

no

fen

ph

os

0.0

35

AA

Dia

zin

on

0.0

11

-0.0

35

A

Dic

hlo

rvo

s0

.01

1-0

.175

A

Dim

eth

oa

te0

.01

1A

Eth

ion

0.0

11

-0.1

75

AA

Ma

lath

ion

0.0

05

A

Me

thid

ath

ion

0.0

11

A

Ph

osa

lone

0.0

21

A

Pirim

iph

os m

eth

yl

0.0

35

AA

Pro

fen

op

ho

s0

.02

1-0

.10

5A

A

Pro

thio

ph

os

Qu

ina

lph

os

0.0

11

-0.0

35

AA

To

lclo

ph

os m

eth

yl

0.0

11

-0.0

36

AA

De

term

ina

tio

n o

f

Org

an

op

ho

sp

ho

rus

Pe

sticid

es b

y G

as

Ch

rom

ato

gra

ph

y

Me

tho

d 9

85

.22

, A

OA

C

16

th E

d.

(19

95

)

Bro

wn

pa

pe

r /

pla

stic

Am

bie

nt

Te

mp

era

ture

To

tal C

S2

Fre

sh

Fru

its &

Ve

ge

tab

les

1 k

g

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

OrganophosporusCS2

F0

4-0

15

DO

C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

Th

e D

ete

rmin

atio

n

of

Dith

ioca

rba

ma

tes

Pe

sticid

eIn

Fru

its

An

d V

eg

eta

ble

s

usi

ng H

eadsp

ace

Gas

Ch

rom

ato

gra

ph

y

with

Ele

ctr

on

Ca

ptu

re D

ete

ctio

n

jad

ua

l 1

.3

resid

u r

ac

un

per

osa

k

Page 23: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

21

4,4

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AF

4,4

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AF

AF

AF

4,4

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T0

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AF

AF

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ha

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C0

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AF

AF

AF

Be

ta-B

HC

0.0

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FA

F

Gam

ma-B

HC

0.0

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FA

FA

F

De

lta

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C0

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AF

AF

AF

Ald

rin

0.1

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FA

FA

F

Alp

ha

-ch

lord

an

e0

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AF

Ga

mm

a-c

hlo

rda

ne

0.0

5A

F

Die

ldrin

0.0

5A

FA

FA

F

En

dri

n0

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AF

AF

He

pta

ch

lor

0.0

5A

FA

FA

F

He

pta

ch

lor

ep

oxid

e0

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AF

F0

4-0

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De

term

ina

tio

n o

f

Ca

rba

ma

te In

Fru

it

an

d V

eg

eta

ble

s

Usin

g H

igh

Pe

rfo

rma

nce

Liq

uid

Ch

rom

ato

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ph

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Me

tho

d M

an

ua

l fr

om

Wa

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Alli

an

ce

Syste

m

for

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rba

ma

te A

na

lysis

Ald

icarb

Fru

it a

nd

Ve

ge

tab

les

1 k

g0

.01

Bro

wn

Pa

pe

r /

Pla

stic

Am

bie

nt

Te

mp

era

ture

0.0

1 m

g/k

g

2011

Sta

nd

ard

Me

tho

ds o

f

An

aly

sis

of

the

Asso

cia

tio

n o

f O

ffic

ial

An

aly

tica

l C

he

mis

ts,

17

th e

d.

Vo

l 1

.

Me

at,

Pra

wn

,

Sq

uid

& F

ish

F0

4-0

17

De

term

ina

tio

n o

f

Org

an

och

lori

ne

Pe

sticid

es in

Mu

scle

usin

g G

as

Ch

rom

ato

gra

phy

Organochlorine

1 k

gP

lastic

Fro

ze

n

Re

fer

to

Six

tee

nth

Sch

ed

ule

(Re

gu

latio

n

41

)

DO

C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

CO

NT

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ER

TR

AN

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OR

TA

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N

ST

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UM

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SID

UE

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ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

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MKA KK

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SELANGOR

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ua

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osa

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Page 24: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

22

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term

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f

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sticid

e R

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in T

ea

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EC

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tho

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term

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in L

ow

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ER

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fer

to 1

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ed

ule

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gu

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n

41

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urn

al o

f A

OA

C

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rna

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na

l

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l. 8

6,

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. 2

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urn

al o

f A

OA

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Inte

rna

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na

l V

ol. 8

6,

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. 2

: 4

12

-43

1

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it a

nd

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ge

tab

les

1 k

g

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wn

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pe

r /

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stic

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bie

nt

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mp

era

ture

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fer

to 1

6

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ed

ule

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gu

latio

n

41

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a5

00

g

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wn

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pe

r /

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stic

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bie

nt

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mp

era

ture

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C.

NO

TE

ST

ME

TH

OD

GROUP

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(m

g/k

g)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

RE

SID

UE

LIM

ITS

(MR

Ls)

in f

oo

d

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

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jad

ua

l 1

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un

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osa

k

Page 25: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

23

jad

ua

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bio

tek

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gi

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ka

na

n

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N

ST

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AG

E

MKAK

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MKA KK

KUCHING

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G0

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ini K

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i

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aw

ma

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plic

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alit

ative

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y s

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urc

ha

se

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Page 26: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

24

G0

4-0

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MS

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rig

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SP

OR

TA

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N

ST

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AG

E

MKAK

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MKA KK

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SELANGOR

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Raw

:

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g

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jad

ua

l 1

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bio

tek

no

lo

gi

ma

ka

na

n

Page 27: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

25

G0

4-0

15

Qu

alit

ative

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aly

sis

of

Ne

wL

ea

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in

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d P

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to P

rod

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stin

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or

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du

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co

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kits A

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cre

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Sp

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ST

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MKA KK

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SELANGOR

PAHANG

KELANTAN

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jad

ua

l 1

.4

bio

tek

no

lo

gi

ma

ka

na

n

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26

G0

4-0

24

Qu

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ative

An

aly

sis

of

Ma

ize

T2

5 in

Corn

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rne

ls a

nd

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rn

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gfo

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mb

ina

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A

Te

ch

niq

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nsla

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n b

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HL

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Ma

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T2

5D

ete

ctio

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ern

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an

d c

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ba

se

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du

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Ke

rne

ls :

Min

. 2

kg

Pro

du

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:

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ack,

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.

20

0g

/pa

ck

0.1

%

G0

4-0

25

De

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ub

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bu

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NA

in

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l

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su

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ea

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rod

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kits A

nim

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du

cts

fo

r th

e

pre

se

nce

of

An

ima

l

Sp

ecie

s a

nd

Jo

urn

al

of

Da

iry R

ese

arc

h

(20

01

) 6

8 U

se

of

Du

ple

x-P

CR

Te

ch

niq

ue

to

Id

en

tify

Bo

vin

e a

nd

Wa

ter

Bu

ffa

lo M

ilku

se

d in

Ma

kin

g M

ozza

rella

Ch

ee

se

Bu

ba

lus b

ub

alis

De

tectio

n

An

ima

l tissu

e

an

d f

oo

d

pro

du

cts

Anim

al T

issue:

1 k

g F

ood

Pro

ducts

: 250g

G0

4-0

26

DN

A E

xtr

actio

n f

rom

Ed

ible

Fa

t u

sin

g

Ep

ice

ntr

e K

it

Use

rM

an

ua

l fo

r th

e

Exra

ctio

n o

f D

NA

fro

m

Fo

od

s

Extr

actio

n m

ilk

& m

ilkp

rod

ucts

an

d e

dib

le f

at

No

t

Ap

plic

ab

le

Milk

& m

ilk

pro

du

cts

an

d

ed

ible

fa

t

Pro

du

cts

:

2 p

acks,

Min

.

20

0g

/pa

ck

No

t

Ava

ilab

le

An

y s

uita

ble

co

nta

ine

r o

r

orig

ina

l

pa

cka

gin

g

As p

urc

ha

se

d

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

ME

TH

OD

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.4

bio

tek

no

lo

gi

ma

ka

na

n

Page 29: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

27

jad

ua

l 1

.5

cem

ar

an

lo

ga

m b

er

at

DO

C.

NO

TE

ST

ME

TH

OD

P

AR

AM

ET

ER

PA

RA

ME

TE

RF

OO

D

MA

TR

IX

MIN

IMU

M

WE

IGH

T

LO

Q

(mg

/kg

)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

H0

4-0

01

Th

e D

ete

rmin

atio

n o

f

Me

rcu

ry in

Fo

od

by

Ato

mic

Ab

so

rptio

n

Sp

ectr

om

ete

r -

Flo

w

Inje

ctio

n A

na

lysis

Syste

m (

AA

S-F

IAS

)

MS

95

4 :

Pa

rt 1

3,

19

89

To

talM

erc

ury

Fis

h a

nd

fish

pro

du

ct

/ sh

ellf

ish

1 k

g

(with

sh

ell)

0.0

7

Pre

da

tory

: 1

,

Oth

er

Fis

h :

0.5

,

Oth

er

Fo

od

Ma

tric

es :

0.0

5

AF

AF

Plu

mb

um

0.7

50

.1 -

2*

AF

Ca

dm

ium

0.0

71

AF

AF

To

tal A

rse

nic

10

.1 -

1*

Sta

nu

m1

0

Pa

cke

d w

ith

ca

n o

r tin

fo

il:

25

0,

Oth

ers

:4

0A

F

Plu

mb

um

0.0

40

.1 -

2*

AA

F

Ars

en

ic0

.20

.1 -

1*

Ca

dm

ium

0.1

1

Plu

mb

um

0.7

50

.2 -

2*

A

Ca

dm

ium

0.2

51

AF

AA

H0

4-0

05

Th

e D

ete

rmin

atio

n o

f

Me

rcu

ry in

Fo

od

by

Ato

mic

Ab

so

rptio

n

Sp

ectr

op

ho

tom

etr

y

(AA

S)

Co

ld V

ap

ou

r

Acce

sso

rie

s (

AV

A)

Fo

od

Qu

alit

y C

on

tro

l

Div

isio

n,

19

97

. T

he

De

term

ina

tio

n o

f

Me

rcu

ry in

Fo

od

an

d

Blo

od

by A

tom

ic

Sp

ectr

om

etr

y (

AA

S)

usin

g a

n A

tom

ic V

ap

or

Acce

sso

ry.

Me

tho

d

5.3

.2

To

talM

erc

ury

Fis

h a

nd

fish

pro

du

ct

/ sh

ellf

ish

1 k

g (

with

sh

ell)

0.0

3

Pre

da

tory

: 1

,

Oth

er

Fis

h :

0.5

,

Oth

er

Fo

od

Ma

tric

es :

0.0

5

AF

H0

4-0

03

H0

4-0

04

50

0 g

/ml

50

0 g

/ml

Th

e D

ete

rmin

atio

n o

f

Plu

mb

um

, C

ad

miu

m a

nd

Ars

en

ic in

Fo

od

by

Gra

ph

ite

Fu

rna

ce

Ato

mic

Ab

so

rptio

n

Sp

ectr

op

ho

tom

ete

r

(GF

AA

S)

AO

AC

99

9.1

0,

20

00

AO

AC

25

.10

7,

19

84

AO

AC

25

.10

7,

19

84

Pe

rish

ab

le

an

d n

on

-

pe

rish

ab

le

foo

d

All

typ

e o

f

foo

d

exce

pt

sa

lt,

oil

& f

at

Th

e D

ete

rmin

atio

n o

f

He

avy

Me

tal in

Fo

od

by

Ind

uctive

ly C

ou

ple

d

Pla

sm

a -

Op

tica

l

Em

issio

n S

pe

ctr

om

ete

r

(IC

P-O

ES

)

H0

4-0

02

Pe

rish

ab

le

an

d n

on

-

pe

rish

ab

le

foo

d

Pla

stic /

orig

ina

l

pa

cka

gin

g

Ch

ill a

nd

fro

ze

n

co

nd

itio

n t

ran

sp

ort

ed

with

in 2

4 h

ou

rs

50

0 g

/ml

Th

e D

ete

rmin

atio

n o

f

Plu

mb

um

an

d C

ad

miu

m

in F

oo

d b

y A

tom

ic

Ab

so

rptio

n

Spectr

ophoto

metr

y (A

AS

)

Page 30: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

28

H0

4-0

08

Th

e D

ete

rmin

atio

n o

f

He

avy

Me

tals

In F

oo

d

Usin

g In

du

ctively

Co

up

led

Pla

sm

a-M

ass

Sp

ectr

om

etr

y (

ICP

-MS

)

AO

AC

99

9.1

0,

20

00

Ca

dm

ium

Fis

h a

nd

Fis

h

Pro

du

cts

1 k

g1

0 u

g/k

g

Pla

stic /

Ori

gin

al

Pa

cka

gin

g

Ch

illa

nd

fro

ze

n

co

nd

itio

n t

ran

sp

ort

ed

with

in 2

4 h

ou

rs

50

ug

/kg

A

Ca

dm

ium

Plu

mb

um

25

mg

/kg

AO

AC

99

9.1

0,

20

00

Am

bie

nt

Te

mp

era

ture

10

mg

/kg

(Ja

pa

n

Sta

nd

ard

)

H0

4-0

09

Th

e D

ete

rmin

atio

n o

f

Plu

mb

um

an

d C

ad

miu

m

In P

lastic F

oo

d C

on

tact

ma

teri

al b

y U

sin

g

Ind

uctive

ly C

ou

ple

d

Pla

sm

a-O

ptica

l E

mis

sio

n

Sp

ectr

om

ete

r

(IC

P-O

ES

)

Pla

stic

Fo

od

Co

nta

ct

ma

teri

al

10

0g

As p

urc

ha

se

d

DO

C.

NO

TE

ST

ME

TH

OD

P

AR

AM

ET

ER

PA

RA

ME

TE

RF

OO

D

MA

TR

IX

MIN

IMU

M

WE

IGH

T

LO

Q

(mg

/kg

)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

(mg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.5

cem

ar

an

lo

ga

m b

er

at

Page 31: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

29

j

ad

ua

l 1

.6

sta

nd

ar

d d

an

pela

bela

n m

ak

an

an

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

RE

GU

LA

TO

RY

LIM

IT

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

J0

4-0

02

De

term

ina

tio

n o

f

Mo

istu

re in

Fo

od

usin

g

Dry

ing

Te

ch

niq

ue

(Co

nve

ntio

na

la

nd

Va

cu

um

Ove

n)

Mo

istu

reA

J0

4-0

03

De

tem

ina

tio

n o

f A

sh

in

Fo

od

Mu

ffle

Fu

rna

ce

Ash

A

J0

4-0

04

De

term

ina

tio

n o

f P

rote

in

in F

oo

d U

sin

g K

jeld

ah

l

Te

ch

niq

ue

Pro

tein

A

J0

4-0

05

De

term

ina

tio

n o

f F

at in

So

yb

ea

n S

au

ce

usin

g

Liq

uid

-Liq

uid

Extr

actio

n

Te

ch

niq

ue

J0

4-0

06

De

term

ina

tio

n o

f F

at in

Fo

od

usin

g A

cid

Hyd

rolis

is T

ech

niq

ue

J0

4-0

07

De

term

ina

tio

n o

f F

at in

Milk

an

d M

ilk P

rod

ucts

usin

g R

oe

se

Go

tlie

b

Me

tho

d

J0

4-0

09

De

term

ina

tio

n o

f F

at in

Dry

Fo

od

usin

g S

oxh

let

Te

ch

niq

ue

J0

4-0

10

De

term

ina

tio

n o

f F

at in

We

t F

oo

d u

sin

g S

oxh

let

Te

ch

niq

ue

J0

4-0

11

De

term

ina

tio

n o

f F

at in

Hig

h S

ug

ar

Fo

od

usin

g

So

xh

let

Te

ch

niq

ue

J0

4-0

12

De

term

ina

tio

n o

f F

at in

Sa

lad

Dre

ssin

g S

am

ple

usin

g C

ott

on

an

d

So

xh

let

Te

ch

niq

ue

50

0g

No

t

Ava

ilab

le

Ori

gin

al

pa

cka

gin

gA

s p

urc

ha

se

Re

fer

to

Fo

od

Re

gu

latio

ns

19

85

Fa

t

Ba

se

d O

n T

rain

ing

Ma

teri

al P

rovid

ed

by

JIC

A's

Exp

ert

(2

00

4)

extr

acte

d f

rom

An

aly

tica

l

Ma

nu

alfo

r S

tan

da

rd

Ta

ble

s o

f F

oo

d

Co

mp

ositio

n in

Ja

pa

n,

5th

Re

vis

ed

Ed

itio

n

(20

00)

Pre

pa

red

ce

rea

l fo

od

bre

ad

milk

cu

ltu

red

milk

flo

ur

co

nfe

ctio

n

ca

nn

ed

me

at

ca

nn

ed

me

at

with

oth

er

foo

d

ca

nn

ed

fish

ca

nn

ed

ve

ge

tab

les

ca

nn

ed

fru

its

fru

it ju

ice

sa

lad

dre

ssin

g

ma

yo

nn

ais

e

so

ft d

rin

ks

Page 32: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

30

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

RE

GU

LA

TO

RY

LIM

IT

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

J0

4-0

13

Ove

rall

Ca

lcu

latio

n a

nd

Inte

rpre

tatio

n o

f

Pro

xim

ate

An

aly

sis

in

Fo

od

Sa

mp

les

An

aly

tica

l M

an

ua

lfo

r

Sta

nd

ard

Ta

ble

s o

f F

oo

d

Co

mp

ositio

n in

Ja

pa

n,

5th

Re

vis

ed

Ed

itio

n,

20

00

Ca

rbo

hyd

rate

,

En

erg

y

J0

4-0

14

De

term

ina

tio

n T

ota

l

Die

tary

Fib

re in

Fo

od

AO

AC

In

tern

atio

na

l,

16

th E

ditio

n,

Vo

lum

eII,

Se

ctio

n 4

5.4

.07

,

Me

tho

d 9

85

.29

(1

99

7)

To

tal D

ieta

ry

Fib

er

J0

4-0

15

Th

e D

ete

rmin

atio

n o

f

Nitro

ge

n u

sin

g

KJE

LD

AH

LM

eth

od

Pe

ars

on

's C

he

mic

al

An

aly

sis

of

Fo

od

s.

8th

Ed

itio

nP

rote

in

Ori

gin

al

pa

cka

gin

gA

s p

urc

ha

se

Re

fer

to

Fo

od

Re

gu

latio

ns

19

85

Pre

pa

red

ce

rea

lfo

od

bre

ad

milk

cu

ltu

red

milk

flo

ur

co

nfe

ctio

n

ca

nn

ed

me

at

ca

nn

ed

me

at

with

oth

er

foo

d

ca

nn

ed

fish

ca

nn

ed

ve

ge

tab

les

ca

nn

ed

fru

its

fru

it ju

ice

sa

lad

dre

ssin

g

ma

yo

nn

ais

e

so

ft d

rin

ks

50

0g

No

t

Ava

ilab

le

j

ad

ua

l 1

.6

sta

nd

ar

d d

an

pela

bela

n m

ak

an

an

Page 33: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

31

jad

ua

l 1

.7

mik

ro

bio

lo

gi

ma

ka

na

n

DO

C.N

OT

ES

TM

ET

HO

DP

AR

AM

ET

ER

TE

CH

NIQ

UE

LO

Q

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

PERLIS

P. PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

SANDAKAN

MIRI

K04-0

01-0

3S

tandard

Pla

te C

ount -P

our

Pla

te T

echniq

ue

Sta

ndard

Pla

te C

ount

Enum

era

tion

10 C

FU

/gA

AA

AA

AA

AA

AA

A

K04-0

02-0

3Y

easts

&M

ould

Countin

Food -

Surf

ace S

pre

ad

Yeast &

mould

Enum

era

tion

100 C

FU

/gA

K04-0

03-0

3E

xam

inatio

n o

fC

olif

orm

s a

nd E

scherichia

coli

-

MP

N T

echniq

ue

Colif

orm

&

Escherichia

coli

Enum

era

tion

3 M

PN

/g (

food),

1 M

PN

/100 m

l

(wate

r)

AA

AA

AA

AA

AA

AA

A

K04-0

05-0

3E

xam

inatio

n o

f C

oagula

se p

ositi

ve S

taphyl

ococci-

Spre

ad P

late

Techniq

ue

Coagula

se P

ositi

ve

Sta

phyl

ococci

Enum

era

tion

100 C

FU

/gA

AA

AA

AA

AA

AA

AA

K04-0

08-0

3E

xam

inatio

n o

fS

alm

onella

eS

alm

onella

Dete

ctio

n0.0

4 C

FU

/gA

AA

AA

AA

AA

AA

A

K04-0

07-0

3E

xam

inatio

n o

fB

acill

us c

ere

us

Bacill

us

cere

us

Enum

era

tion

100 C

FU

/gA

AA

AA

AA

AA

AA

AA

K04-0

03-0

2E

.coli/

Colif

orm

Count P

late

s-

3M

™P

etr

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scherichia

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colif

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era

tion

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FU

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AF

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AA

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A

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01-0

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bic

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late

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late

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east and M

ould

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3M

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etr

ifilm

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mould

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era

tion

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FU

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K04-0

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xam

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specifi

corg

anis

ms –

Vib

rio

Para

haem

oly

ticus

Vib

rio

para

haem

oly

ticus

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era

tion

3M

PN

/gA

FA

A

K04-0

09-0

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ete

ctio

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fV

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hole

rae

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nd 0

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cessed

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or

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hole

rae

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FU

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unoassay

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CR

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ET

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nD

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n-

Page 34: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

32

jad

ua

l 1

.7

mik

ro

bio

lo

gi

ma

ka

na

n

K04-0

05-0

5S

taphylo

coccal E

nte

roto

xin

Vis

ual Im

munoassa

y

(TE

CR

A M

ET

HO

D)

Sta

phylo

coccal to

xin

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ction

-

K04-0

14-0

3E

xam

ination for

specific

org

anis

ms-C

am

pylo

bacte

r C

am

pylo

bacte

rD

ete

ction

0.0

4 C

FU

/gA

2011

K04-0

13-0

4D

ete

ction o

f Lis

teria M

onocyto

genes

Lis

teria

monocyto

genes

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ction

0.0

4 C

FU

/gA

A

K04-0

06-0

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num

era

tion o

f F

aecal S

trepto

cocci-S

pre

ad

Pla

te T

echniq

ue

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trepto

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era

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n-

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05-0

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taph E

xpre

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ount P

late

- 3M

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etr

ifilm

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AA

AA

A

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17-0

3E

num

ara

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f C

lostr

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m p

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ringens in

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urf

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read T

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f P

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acill

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t 30

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FU

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)E

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acill

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FU

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ilk a

nd

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C.

NO

TE

ST

ME

TH

OD

P

AR

AM

ET

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TE

CH

NIQ

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LO

Q

MKAK

MKA IPOH

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TERENGGANU

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MIRI

Page 35: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

33

K0

4-0

15

-06

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um

era

tio

n o

f E

nte

rob

acte

r sa

ka

za

kii

in M

ilk

an

d M

ilk P

rod

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En

tero

ba

cte

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sa

ka

za

kii

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um

era

tio

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FU

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K0

4-0

19

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(2)

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tio

n o

f S

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sp

p.

Sh

ige

lla s

pp

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nu

me

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00

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ctic A

cid

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um

era

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FU

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19

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tectio

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pp

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ou

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ou

nt

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wa

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ou

ld C

ou

nt

En

um

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n-

K0

4-0

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-04

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era

tion o

f Lactic

Acid

Bacte

ria in

Milk

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duct-

Su

rfa

ce

Sp

rea

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ech

niq

ue

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actic A

cid

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ast

an

d M

ou

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in F

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mp

act

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su

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ea

st

& m

ou

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me

ratio

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U/g

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C.N

OT

ES

TM

ET

HO

DP

AR

AM

ET

ER

TE

CH

NIQ

UE

LO

Q

MKAK

MKA IPOH

MKA JB

MKA KK

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SANDAKAN

MIRI

En

um

era

tio

n o

f L

actic A

cid

Ba

cte

ria

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lon

y

Co

un

t T

ech

niq

ue

at

30

C

o

jad

ua

l 1

.7

mik

ro

bio

lo

gi

ma

ka

na

n

Page 36: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

34

jad

ua

l 1

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em

ar

an

mik

olo

gi

DO

C.

NO

TE

ST

ME

TH

OD

PA

RA

ME

TE

RP

AR

AM

ET

ER

FO

OD

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TR

IX

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M

WE

IGH

T

LO

D

(µg/k

g)

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NT

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ER

TR

AN

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TIO

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ST

OR

AG

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MA

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UM

PE

RM

ITT

ED

PR

OP

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TIO

N

(µg

/kg

)

MKAK

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KEDAH

PERLIS

PULAU PINANG

SELANGOR

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KELANTAN

TERENGGANU

Afla

toxin

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toxin

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20

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10

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20

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n o

f

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rato

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e a

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ea

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sin

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un

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ffin

ity C

olu

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an

Up

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ua

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um

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r 5

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e,

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ea

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ur

&

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co

a

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wd

er

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A

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term

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f

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ffe

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mu

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ua

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kg

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an

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aly

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ua

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toxin

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rea

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35

jad

ua

l 1

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olo

gi

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4-0

08

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f

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ilkb

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KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

Page 38: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

36

L0

4-0

15

De

term

ina

tio

n o

f

De

oxyn

iva

len

ol in

Ric

e,

Ma

ize

an

d W

he

at

Pro

du

ct

by u

sin

g

Imm

on

ua

ffin

ity c

olu

mn

an

d H

PL

C

VIC

AM

DO

NT

est

HP

LC

Instr

uctio

n

Ma

nu

alM

eth

od

Nu

mb

er

4.1

De

oxyn

iva

len

ol

Ce

rea

ls1

kg

80

Ori

gin

al

Pa

cka

gin

g /

Am

be

r G

lass

Bo

ttle

Ro

om

Te

mp

era

ture

5

L0

4-0

16

Qu

an

tita

tive

An

aly

sis

fo

r

Milk

by R

ida

scre

en

Fa

st

Afla

toxin

M1

Kit In

str

uctio

n M

an

ua

lA

fla

toxin

M1

Milk

50

0 m

l0

.5

Ori

gin

al

Pa

cka

gin

g/

Am

be

r P

lastic

Bo

ttle

< 4

0C

fo

r

pa

ste

urise

d m

ilk

(ch

ill)/

Ro

om

Te

mp

era

ture

fo

r

UH

Ta

nd

Ste

riliz

ed

Milk

0.5

DO

C.

NO

TE

ST

ME

TH

OD

PA

RA

ME

TE

RP

AR

AM

ET

ER

FO

OD

MA

TR

IX

MIN

IMU

M

WE

IGH

T

LO

D

(µg/k

g)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

E

MA

XIM

UM

PE

RM

ITT

ED

PR

OP

OR

TIO

N

(µg

/kg

)

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

jad

ua

l 1

.8 c

em

ar

an

mik

olo

gi

Page 39: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

37

jad

ua

l 1

.9 pem

bu

ng

ku

sa

n

DO

C.

NO

TE

ST

ME

TH

OD

STATUSR

EF

ER

EN

CE

PA

RA

ME

TE

RF

OO

DM

AT

RIX

MIN

IMU

M W

EIG

HT

LO

Q

(mg/k

g)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

EM

AX

IMU

M P

ER

MIT

TE

D P

RO

PO

RT

ION

Ja

pa

n S

an

ita

tio

n L

aw

, 1

99

9

1.

To

lue

ne

●S

tyre

ne

= ≤

10

00

mg

/kg

2.

Eth

ylb

en

ze

ne

●E

thylb

en

ze

ne

= ≤

10

00

mg

/kg

3.

iso

-Pro

pylb

en

ze

ne

●T

ota

l co

nce

ntr

atio

n o

f 5

co

mp

ou

nd

s =

4.

n-P

rop

ylb

en

ze

ne

≤ 5

00

0 m

g/k

g

5.

Sty

ren

e

≤ 2

00

0 m

g/k

g (

PS

fo

am

)

≤ 1

50

0 m

g/k

g

(m

ilk &

milk

pd

t)

1.

Ph

en

ol

Ja

pa

n S

an

ita

tio

n L

aw

, 1

99

9

2.

Bis

ph

en

ol A

Ma

teri

al T

est

3.

p-t

Bu

tylp

he

no

l●

Dip

he

nylc

arb

on

te =

≤ 5

00

mg

/kg

4.

Dip

he

nylc

arb

on

ate

●T

ota

l co

nce

ntr

atio

n o

f 3

co

mp

ou

nd

s (

Bis

ph

en

ol A

, P

he

no

l,

p-t

bu

tylp

he

no

l) =

≤ 5

00

mg

/kg

1.

Ph

en

ol

Ja

pa

n S

an

ita

tio

n L

aw

, 1

99

9

2.

Bis

ph

en

ol A

Mig

ratio

n T

est

3.

p-t

Bu

tylp

he

no

lB

isp

he

no

l A

= ≤

2.5

mg

/kg

4.

Dip

he

nylc

arb

on

ate

Sp

ecific

atio

n a

nd

Sta

nd

ard

sfo

r fo

od

s,

the

ir

co

nta

ine

rs a

nd

pa

cka

ge

s

etc

.

(B

ase

d o

n t

he

Fo

od

Sa

nita

tio

n L

aw

),

Ja

pa

n F

oo

d H

yg

ien

e

Asso

cia

tio

n,

19

92

Sp

ecific

atio

n a

nd

Sta

nd

ard

sfo

r fo

od

s,

the

ir

co

nta

ine

rs a

nd

pa

cka

ge

s

etc

.

(B

ase

d o

n t

he

Fo

od

Sa

nita

tio

n L

aw

),

Ja

pa

n F

oo

d H

yg

ien

e

Asso

cia

tio

n,

19

92

● p

acka

ge

with

ou

t fo

od

-

orig

ina

l

co

nta

ine

r /

wra

pp

ed

with

pa

pe

r /

Alu

min

ium

/

hig

h r

esis

tan

t

pla

stic

Ro

om

Te

mp

era

ture

/

Sa

me

Te

mp

era

ture

co

nd

itio

n w

he

n it

is

sam

ple

d

Ro

om

Te

mp

era

ture

/

Sa

me

Te

mp

era

ture

co

nd

itio

n w

he

n it

is

sam

ple

d

MO

H

M0

4-0

03

De

term

ina

tio

n o

f

Bis

ph

en

ol A

, P

he

no

l, p

-t

Bu

thylp

he

no

l a

nd

Dip

he

nylc

arb

on

ate

in

Fo

od

Co

nta

ct

Ma

teri

als

usin

g H

igh

Pe

rfo

rma

nce

Liq

uid

Ch

rom

ato

gra

ph

y

(Mig

ratio

n T

est)

Po

lyca

rbo

na

te

(PC

)

1.

Co

nta

ine

r :

≥ 4

un

its

● p

acka

ge

co

nta

inin

g

foo

d in

co

nta

ct

-

orig

ina

l

co

nta

ine

r

8m

g/k

g

Po

lysty

ren

e

(PS

)

Po

lyca

rbo

na

te

(PC

)

1.

Stirr

er/

sp

oo

n/

fork

/ ch

op

stick :

≥ 5

un

its

2.

Co

nta

ine

r/

pla

tes/

cu

ps/

tra

y :

≥ 2

un

its

1.

Co

nta

ine

r :

≥ 1

un

it

0.5

mg/L

(Phenol, p

-t-

buty

lphenol,

dip

henylc

arb

onate

)

MO

H

M0

4-0

01

10

mg

/kg

3.

Oth

ers

:

≥ 2

un

its

De

term

ina

tio

n o

f

Re

sid

ua

l S

tyre

ne

Mo

no

me

r a

nd

Oth

er

Vo

latile

Org

an

ic

Co

mp

ou

nd

s (

VO

Cs)

in

Fo

od

Co

nta

ct

Ma

teri

als

usin

g G

as

Ch

rom

ato

gra

ph

y

MO

H

M0

4-0

02

De

term

ina

tio

n o

f re

sid

ua

l

Bis

ph

en

ol A

, P

he

no

l, p

-t

Bu

thylp

he

no

l a

nd

Dip

he

nylc

arb

on

ate

in

Fo

od

Sim

ula

nts

usin

g

Hig

h P

erf

orm

an

ce

Liq

uid

Ch

rom

ato

gra

ph

y

(Ma

teria

ln T

est)

Th

e P

ha

rma

ce

utica

l

So

cie

ty o

f Ja

pa

n

(Hyg

ien

e T

est

Me

tho

d

No

te)

A

0.2

mg

/L

(Bis

ph

en

ol A

)

PS6

OT

HE

R

7

OT

HE

R

7

Page 40: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

38

1. D

ieth

yl phath

ala

te (

DE

P)

Po

lysty

ren

e (

PS

)

2. D

i-is

o-p

ropyl phth

ala

te (

DiP

P)

3. D

i-n-p

ropyl phth

ala

te (

DnP

P)

4. D

i-is

o b

uty

l phth

ala

te (

DiB

P)

5. D

i-n-b

uty

l sebacate

(D

BS

)

6. B

uty

l phth

aly

buty

l gly

cola

te

(BP

BG

)

7. D

i-hexyl phth

ala

te (

DH

xP

)

8. D

i-cylo

hexyl phth

ala

te

(DC

HP

)

9. T

ri-n

-buty

l tr

imery

tate

(T

BT

M)

Po

lycarb

on

ate

(P

C)

10. D

i-2-e

thylh

exyl azela

te

(DE

HA

8)

Conta

iner

: 1 u

nit

11. D

imeth

yl phth

ala

te (

DM

P)

12. D

i-n-b

uty

l phth

ala

te (

DnB

P)

Po

lyvin

yl ch

lori

de

(PV

C)

13. D

ipenty

l phth

ala

te (

DP

eP

)&

14. A

cety

l-tr

i-n-b

uty

l citra

te

(AT

BC

)

15. B

uty

l benzyl phth

ala

te (

BB

P)

16. D

i-2-e

thyl hexyl adip

ate

(DE

HA

)C

onta

iner

: 1 u

nit

17. T

ri-2-e

thyl

hexy

l phth

ala

te (T

OP

)

18. D

i-2-e

thylh

exyl phth

ala

te

(DE

HP

)

19. D

i-n-o

cty

l phth

ala

te (

DnO

P)

20. T

ri-2

-eth

ylh

exyl tr

imelli

tate

(TO

TM

)

21. D

i-hepty

l phth

ala

te (

DhpP

)

22. D

i-is

o-n

onyl phth

ala

te (

DIN

P)

AM

OH

M04-

004

Dete

rmin

ation o

f

Pla

sticiz

ers

in F

ood

Conta

ct M

ate

rial usin

g

Gas C

hro

mato

gra

ph

● p

ackage

conta

inin

g

food in

conta

ct -

origin

al

conta

iner

● p

ackage

without fo

od -

origin

al

conta

iner

/

wra

pped w

ith

paper

/

Alu

min

ium

/

hig

h r

esis

tant

pla

stic

Room

Tem

pera

ture

/

sam

e tem

pera

ture

conditio

n w

hen it is

sam

ple

d

Poly

styr

ene (P

S)

Poly

vin

yl

chlo

ride (

PV

C)/

Maste

r T

hesis

of Z

alil

ah

Nasir

2.

Conta

iner/

pla

tes/

cups/ tr

ay :

≥ 2

units

1.

Stirr

er/

spoon/

fork

/ chopstick :

≥ 5

units

3.

Oth

ers

:

≥ 2

units

Poly

carb

onate

(PC

)

40m

g/k

g

Po

lyvin

ylid

ine

Ch

lori

de (

PV

DC

)

Poly

vin

ylid

ine

Chlo

ride (P

VD

C)

Japan S

anitation L

aw

,Code o

f

Federa

l R

egula

tions ,

US

AE

uro

pean L

egis

lation,

EU

(Types o

f banned p

lasticiz

ers

)

DO

C.

NO

TE

ST

ME

TH

OD

STATUS

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

(mg/k

g)

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

EM

AX

IMU

M P

ER

MIT

TE

D P

RO

PO

RT

ION

PV

C3

jad

ua

l 1

.9 pem

bu

ng

ku

sa

n

Page 41: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

39

2

DO

C.

NO

TE

ST

ME

TH

OD

STATUS

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

CO

NT

AIN

ER

TR

AN

SP

OR

TA

TIO

N

ST

OR

AG

EM

AX

IMU

M P

ER

MIT

TE

D P

RO

PO

RT

ION

jad

ua

l 1

.9 pem

bu

ng

ku

sa

n

Page 42: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

40

µ

DO

C.

NO

TE

ST

ME

TH

OD

STATUS

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IXM

INIM

UM

WE

IGH

TL

OQ

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

EM

AX

IMU

M P

ER

MIT

TE

D P

RO

PO

RT

ION

jad

ua

l 1

.9 pem

bu

ng

ku

sa

n

Page 43: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

41

DO

C.

NO

TE

ST

ME

TH

OD

RE

FE

RE

NC

EP

AR

AM

ET

ER

FO

OD

MA

TR

IX

MIN

IMU

M

WE

IGH

T

LO

Q

(mg/k

g)

C

ON

TA

INE

RT

RA

NS

PO

RT

AT

ION

ST

OR

AG

E

RE

GU

LA

TO

RY

LIM

IT

MKAK

MKA IPOH

MKA JB

MKA KK

KUCHING

KEDAH

PERLIS

PULAU PINANG

SELANGOR

PAHANG

KELANTAN

TERENGGANU

Nitrite

Nitra

te

Ch

lorid

e

Bro

mid

e

N0

4-0

03

Th

e D

ete

ctio

n o

f P

ea

nu

t

Alle

rge

n in

Fo

od

by

usin

g A

lert

® P

ea

nu

t

Alle

rge

n S

cre

en

ing

Te

st

Kit In

str

uctio

n M

an

ua

lP

ea

nu

t

Alle

rgen

Pe

an

ut

pro

du

cts

5

N0

4-0

04

Th

e D

ete

rmin

atio

n o

f

Pe

an

ut

Alle

rge

n In

Fo

od

By U

sin

g V

era

tox®

Qu

an

tita

tive

Pe

an

ut

Alle

rge

nT

est

Kit In

str

uctio

n M

an

ua

lP

ea

nu

t

Alle

rgen

Pe

an

ut

pro

du

cts

2.5

N0

4-0

05

Th

e D

ete

ctio

n o

f M

ilk

Alle

rge

n In

Fo

od

Usin

g

Ale

rt®

Milk

Alle

rge

n

Scre

en

ing

Te

st

Kit In

str

uctio

n M

an

ua

lM

ilk A

llerg

en

Milk

pro

du

cts

5

N0

4-0

06

Th

e D

ete

rmin

atio

n o

f

Milk

Alle

rge

n In

Fo

od

Usin

g V

era

tox®

To

tal

Milk

alle

rge

n

Qu

an

tita

tive

Te

st

Kit

Kit In

str

uctio

n M

an

ua

lM

ilk A

llerg

en

Milk

pro

du

cts

2.5

N0

4-0

07

Th

e D

ete

ctio

n o

f E

gg

Alle

rge

n In

Fo

od

Usin

g

Ale

rt® E

gg

Alle

rge

n

Scre

en

ing

Te

st

Kit In

str

uctio

n M

an

ua

lE

gg

Alle

rge

nE

gg

pro

du

cts

5

Ori

gin

al

pa

cka

gin

g5

00

g

5

1 k

g

Ric

e

Ve

ge

tab

les

N0

4-0

02

De

term

ina

tio

n o

f

Ch

lorid

e a

nd

Bro

mid

e in

Ric

e u

sin

g Io

n

Ch

rom

ato

gra

ph

y S

yste

m

US

En

vir

on

me

nta

l

Pro

tectio

n A

ge

ncy

(EP

A M

eth

od

90

56

A

Re

vis

ion

1 F

eb

20

07

)

US

En

vir

on

me

nta

l

Pro

tectio

n A

ge

ncy

(EP

A M

eth

od

90

56

A

Re

vis

ion

1 F

eb

20

07

)

10

Ro

om

Te

mp

era

ture

or

ch

ille

d if

mo

re t

ha

n

24

ho

urs

Ro

om

Te

mp

era

ture

No

Re

gu

latio

n

Re

fer

to F

oo

d

Re

gu

latio

n 1

98

5

Bro

wn

Pa

pe

r

Pla

stic

De

term

ina

tio

n o

f N

itra

te

an

d N

itrite

in

Ve

ge

tab

les

usin

g Io

n

Ch

rom

ato

gra

ph

y S

yste

m

N0

4-0

01

jad

ua

l 1

.10

cem

ar

an

sem

ula

ja

di

Page 44: Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u o ] v ] i o u v P ] v P ] v u v P l } } µ l u l v v Ç v P ... LOQ (gµ/kg) CONTAINER

42

N0

4-0

08

Th

e D

ete

rmin

atio

n O

f

Eg

g A

llerg

en

In

Fo

od

Usin

g V

era

tox®

Qu

an

tita

tive

Eg

g

Alle

rge

n

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